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π§ Dr. Pooja Talks IV Glutathione at Halcyon Aesthetics Dubai! β¨, Ever wondered why Glutathione is called the βmaster antioxidantβ? π¬, Dr. Pooja breaks it downβexplaining how IV Glutathione helps ...
After stirring for 3 hours at room temperature, the DCM was removed in vacuo, then a solution of N- (thien-2-ylmethyl) -1H-pyrazol-3-amine (3.17g, 17.7mmol, 1.2 equiv.) in DCM (15 mL) was added, the mixture was heated under nitrogen in a 110 β oil bath for 17 hours to set up the reaction under nitrogen but to evaporate all DCM to give a pure reaction mixture, the resulting residue was dissolved in DCM, extracted once with water, dried over magnesium sulfate, then partially purified on a 340 g silica column (20% to 80% EtOAc/hexane), the fraction containing the desired product was concentrated, then dissolved in EtOAc (30mL) and heated in an oil bath to 47 β, then pentane (50mL) was added, the solution was then cooled in a-20 β refrigerator for 2 hours, the precipitate was collected by filtration, 2.53g of material of approximately 99% purity were obtained
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Dissecting the mechanism of intracellular Mycobacterium smegmatis growth inhibition by platelet activating factor C-16
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